METHOD FOR PREPARING HYDROGEN-RICH SYNTHESIS GAS BY DEGRADING POLYOLEFIN WASTE PLASTICS AT LOW TEMPERATURE
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United States of America Patent
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Mar 16, 2023
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Nov 16, 2022
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May 29, 2021
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Abstract
A method for preparing hydrogen-rich synthesis gas by degrading waste polyolefin plastics at a low temperature includes the following steps: weighing 1 part by weight of polyolefin waste plastics and 3 parts-80 parts by weight of hydrogen peroxide containing 0.25%-6% of H2O2; feeding the polyolefin waste plastics and the hydrogen peroxide into a hydrothermal reactor, and carrying out the oxidation pretreatment reaction at a reaction temperature of 150° C.-230° C. under a reaction pressure of 0.5 MPa-2 MPa for 30 minutes-90 minutes, and obtaining an aqueous-phase product and a gas-phase product after the reaction is finished; filling another hydrothermal reactor with a mesoporous carbon supported metal-based catalyst, and then introducing the aqueous-phase product into the hydrothermal reactor for a reforming reaction to obtain a hydrogen-rich synthesis gas product. In the whole process, the H2 yield is close to 11 mol/kg plastics, and the H2 concentration in the hydrogen-rich synthesis gas is close to 55%.
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