Hydroxypropyl methyl cellulose phthalate and method for producing the same

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United States of America Patent

PATENT NO 11873351
APP PUB NO 20210130498A1
SERIAL NO

17083617

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Abstract

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There is provided a method for producing hydroxypropyl methyl cellulose phthalate (HPMCP), including an esterification step of reacting hydroxypropyl methyl cellulose with a carboxybenzoylating agent in the presence of an aliphatic carboxylic acid in a kneader reactor equipped with two or more stirring blades rotating around their own axes and orbitally revolving, to obtain a reaction product solution containing HPMCP; a precipitation step of precipitating the HPMCP by mixing the reaction product solution with water to obtain a suspension of the precipitated HPMCP; and a washing and recovery step of washing the HPMCP in the suspension and recovering the washed HPMCP. Further, there is provided HPMCP having yellowness at 20° C. of 10.0 or less, as determined in a 10% by mass solution of the HPMCP in acetone.

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Patent Owner(s)

Patent OwnerAddress
SHIN-ETSU CHEMICAL CO LTD6-1 OHTEMACHI 2-CHOME CHIYODA-KU TOKYO 100-0004

International Classification(s)

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  • 2020 Application Filing Year
  • C08B Class
  • 312 Applications Filed
  • 139 Patents Issued To-Date
  • 44.56 % Issued To-Date
Click to zoom InYear of Issuance% of Matters IssuedCumulative IssuancesYearly Issuances2020202120222023202420250255075100

Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kitaguchi, Taishi Niigata, JP 13 4
Matsubara, Junichi Niigata, JP 28 48
Yoshida, Mitsuhiro Niigata, JP 104 849

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Citation count rangeNumber of patents cited in rangeNumber of patents cited in various citation count ranges545901 - 100255075100125150175200225250275300325350375400425450475500525550575

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