Manufacture of hydrophobized nanocellulose intermediate as well as hydrophobized nanocellulose
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United States of America Patent
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Nov 16, 2021
Grant Date -
May 21, 2020
app pub date -
Jun 18, 2018
filing date -
Jun 16, 2017
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Abstract
The present invention relates to a method for manufacturing hydrophobized nanocellulose comprising the steps of: a) providing a cellulose-containing material wherein the cellulose-containing material contains less than 20 wt. % water, b) contacting the cellulose-containing material with oxalic acid dihydrate, and heating above the melting point of the oxalic acid dihydrate, to obtain cellulose oxalates, c) washing the mixture, d) preparing a suspension comprising the material from step c) and e) recovering hydrophobized nanocellulose from the suspension. The present invention relates also to a method of manufacturing hydrophobized nanocellulose intermediate which comprises the above described steps a)-c). The methods disclosed in the present invention are quick, inexpensive, simple, and direct. Pulp can be used as raw material.
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