Dye doped polymer microparticles

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United States of America Patent

PATENT NO 10669360
APP PUB NO 20180244814A1
SERIAL NO

15964735

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Abstract

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Various embodiments provide dye-doped polystyrene microspheres generated using dispersion polymerization. Polystyrene microspheres may be doped with fluorescent dyes, such as xanthene derivatives including Kiton Red 620 (KR620), using dispersion polymerization. Certain functionalities, such as sodium styrene sulfonate, may be used to shift the equilibrium distribution of dye molecules to favor incorporation of the dye into the particles. Polyelectrolyte materials, such as poly(diallyldimethyl ammnonium chloride), PolyDADMAC, may be used to electrostatically trap and bind dye molecules within the particles. A buffer may be used to stabilize the pH change of the solution during dye-doped polystyrene microsphere generation and the buffer may be selected depending on the pKa of the dye being incorporated. The various embodiments may provide dye-doped polystyrene microspheres, such as KR620-doped polystyrene microspheres that are non-toxic and non-carcinogenic. These non-toxic and non-carcinogenic dye-doped polystyrene microspheres may be suitable for use in wind tunnel testing.

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UNITED STATES OF AMERICA AS REPRESENTED BY THE ADMINISTRATOR OF NASA300 E STREET SW WASHINGTON DC 20546

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  • 2018 Application Filing Year
  • C09K Class
  • 2902 Applications Filed
  • 1876 Patents Issued To-Date
  • 64.65 % Issued To-Date
Click to zoom InYear of Issuance% of Matters IssuedCumulative IssuancesYearly Issuances201820192020202120222023202420250255075100

Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Danehy, Paul M Newport News, US 10 20
Danley, Jason E Lincoln, US 2 0
Tiemsin, Pacita I Newport News, US 3 0
Wohl,, Jr Christopher J Portsmouth, US 19 58

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Citation count rangeNumber of patents cited in rangeNumber of patents cited in various citation count ranges706659319301 - 1011 - 2021 - 3031 - 40050100150200250300350400450500550600650700750

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