CONTINUOUS ADIABATIC INVERSE EMULSION POLYMERIZATION PROCESS
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United States of America Patent
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Jul 19, 2018
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Jan 23, 2018
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Jul 24, 2015
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The present invention provides methods and systems for continuous polymerization of ethylenically unsaturated monomers in a water-in-oil inverse emulsion under adiabatic conditions without the need for external cooling during the polymerization. The method comprises neutralizing a monomer composition comprising at least one acidic vinyl monomer with a base in an aqueous medium comprising water and water ice to form an aqueous monomer solution therefrom; homogenizing and degassing to form an inverse monomer emulsion; initiating polymerization; passing the inverse emulsion through a tube reactor without cooling, and flash evaporating a portion of the water from inverse emulsion to cool and concentrate the resulting polymer-containing inverse emulsion. During neutralization, the aqueous medium comprises an amount of water ice sufficient to maintain a temperature of 30° C. or less, and the polymerization is initiated by adding a free-radical polymerization initiator to the emulsion prior to passing the emulsion through the tube reactor.
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