METHOD FOR PRODUCING NICKEL MICROPARTICLES
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United States of America Patent
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Jul 25, 2017
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Sep 12, 2012
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Abstract
The present invention addresses the problem of providing a method for producing nickel microparticles in which the ratio of crystallite's diameter to the particle diameter of the nickel microparticles is controlled. At least two types of fluids to be processed are used, including a nickel compound fluid in which a nickel compound is dissolved in a solvent, and a reducing agent fluid in which a reducing agent is dissolved in a solvent. Sulfate ions are included in the nickel compound fluid, and polyol is included in the nickel compound fluid and/or the reducing agent fluid. The fluid to be processed is mixed in a thin film fluid formed between at least two processing surfaces (1, 2), at least one of which rotates relative to the other, and which are disposed facing each other and capable of approaching and separating from each other, and nickel microparticles are precipitated. The present invention is characterized in that at this time, the ratio (d/D) of crystallite's diameter (d) to the particle diameter (D) of the nickel microparticle is controlled by controlling the pH of the nickel compound fluid introduced between the processing surfaces (1, 2) and the molar ratio of sulfate ions with respect to nickel in the nickel compound fluid.
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