Textured-crystal nanoparticles from ligated anionic element reagent complex
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United States of America Patent
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Oct 27, 2020
Grant Date -
Sep 21, 2017
app pub date -
Mar 21, 2016
filing date -
Mar 21, 2016
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Abstract
A method for synthesizing a reagent complex includes a step of ball-milling a mixture that includes: a powder of a zero-valent element; a hydride molecule; and a nitrile ligand. The method produces a reagent complex having a formula Q0.Xy.Lz, where Q0 is the zero-valent element, X is the hydride molecule, and L is the nitrile ligand. A process for synthesizing nanoparticles composed of the zero-valent element includes a step of adding solvent to the reagent complex. Crystal texture of the nanoparticles is modulated by appropriate selection of the molar ratio nitrile ligand in the reagent complex.
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