NEW CRYSTAL FORM OF PANTOPRAZOLE SODIUM COMPOUND AND PREPARATION METHOD THEREFOR
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United States of America Patent
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Nov 20, 2015
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Feb 12, 2015
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Abstract
A novel crystalline form is defined by using diffraction angle 2θ° of X-ray powder diffraction pattern and characteristic peaks of differential scanning calorimetry (DSC). Pantoprazole Sodium solid is added to an alcohol solvent to form a suspension with a concentration of 0.05˜0.2 g/mL, and then an antioxidant is added to the suspension, completely dissolving the solid at a temperature of 15˜35° C., and a solventing-out agent is dropwise added to the solution under the application of ultrasonic wave, wherein the amount of the solventing-out agent is 3˜10 times (in volume) of the alcohol solvent; followed by cooling the solution down to 0˜5° C., continuing to stir for 1˜3 h, and suction filtrating obtained solid-liquid suspension to provide a novel crystalline form of Pantoprazole Sodium crystal after drying the product to constant weight.
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- 15 United States
- 10 France
- 8 Japan
- 7 China
- 5 Korea
- 2 Other
Patent Owner(s)
Patent Owner | Address | |
---|---|---|
TIANJIN UNIVERSITY | 300072 TIANJIN CITY NANKAI DISTRICT WEI JIN ROAD NO 92 TIANJIN CITY TIANJIN CITY 300072 | |
HAINAN LINGKANG PHARMACEUTICAL CO LTD | NO 16 YAOGU ERHENG ROAD YAOGU INDUSTRIAL PARK HAIKOU NATIONAL HIGH TECH INDUSTRIAL DEVELOPMENT ZONE HAIKOU CITY HAINAN PROVINCE 570318 HAIKOU CITY HAINAN 570318 |
International Classification(s)
Inventor(s)
Inventor Name | Address | # of filed Patents | Total Citations |
---|---|---|---|
HAO, Hongxun | Tianjin, CN | 7 | 0 |
# of filed Patents : 7 Total Citations : 0 | |||
HOU, Baohong | Tianjin, CN | 13 | 0 |
# of filed Patents : 13 Total Citations : 0 | |||
JIANG, Shen | Tianjin, CN | 14 | 3 |
# of filed Patents : 14 Total Citations : 3 | |||
LV, Jun | Haikou, Hainan, CN | 24 | 94 |
# of filed Patents : 24 Total Citations : 94 | |||
TAO, Linggang | Haikou, Hainan, CN | 15 | 0 |
# of filed Patents : 15 Total Citations : 0 | |||
WANG, Jingkang | Tianjin, CN | 20 | 23 |
# of filed Patents : 20 Total Citations : 23 | |||
WANG, Yongli | Tianjin, CN | 23 | 41 |
# of filed Patents : 23 Total Citations : 41 | |||
WANG, Zhao | Tianjin, CN | 240 | 2466 |
# of filed Patents : 240 Total Citations : 2466 | |||
XIE, Chuang | Tianjin, CN | 8 | 27 |
# of filed Patents : 8 Total Citations : 27 | |||
XU, Zhao | Tianjin, CN | 29 | 70 |
# of filed Patents : 29 Total Citations : 70 | |||
YIN, Qiuxiang | Tianjin, CN | 9 | 0 |
# of filed Patents : 9 Total Citations : 0 |
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