MANUFACTURING METHOD OF SILATRANE WITH THIOL GROUP AND PRESERVATION METHOD THEREOF
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United States of America Patent
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app pub date -
Sep 16, 2015
filing date -
Mar 9, 2015
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Abstract
A manufacturing method of silatrane with thiol group and a preservation method thereof are disclosed. (3-Mercaptopropyl)trimethoxysilane and triethanolamine are reacted for a pre-determined time at a pre-determined temperature under nitrogen atmosphere in presence or absence of catalyst, and then a recrystallization process is performed with a solvent to obtain silatrane with thiol group of formula (1). Silatrane with thiol group is dissolved in an organic solvent to preserve the silatrane with thiol group.
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