PREPARATION METHOD FOR MOISTURE-CURING POLYURETHANE REACTIVE HOT MELT ADHESIVE FOR TEXTILE COMPOSITION

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United States of America Patent

SERIAL NO

14917393

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Abstract

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A preparation method for moisture-curing polyurethane reactive hot melt adhesive for textile lamination mainly includes the following steps: (1) mixing and stirring polyether polyol 4000E, polyester polyol 3000H, polyester polyol 2000N, and an antioxidant, heating the mixture to about 120° C., and dehydrating for 0.5h under a vacuum of lower than 100 Pa; (2) adding a tackifying resin, heating the mixture to 135-140° C., and dehydrating for 1.5h under a vacuum of lower than 100 Pa; (3) lowering the temperature to 87° C., adding 4,4′-diphenylmethane diisocyanate and a catalysis, stirring the mixture, and reacting for 2h under a vacuum of lower than 100 Pa; (4) releasing vacuum, adding white carbon black, rapidly stirring the mixture evenly, and further stirring for 10 min under a vacuum of lower than 100 Pa; and (5) rapidly discharging at a temperature of 85-100° C., packaging, and then curing for 4h at 80-85° C., to obtain a target product. When applied in textile lamination, the product exhibits excellent peel strength, a relatively short open time, good hydrolysis resistance and desirable storage stability.

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Patent Owner(s)

Patent OwnerAddress
EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGYSHANGHAI 200237
SHANGHAI TIANYANG HOT MELT ADHESIVE CO LTD505 HUIPING ROAD JIADING DISTRICT SHANGHAI 201802
KUNSHAN TIANYANG HOT MELT ADHESIVE CO LTDQIANDENG TOWN WENPU ROAD KUNSHAN CITY SUZHOU CITY JIANGSU PROVINCE 215341 NO 366 SUZHOU CITY JIANGSU PROVINCE 215341

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
LI, Zhelong Shanghai, CN 10 6
MA, Hongwei Shanghai, CN 86 273
SHEN, Yan Shanghai, CN 51 608
XIAO, Hupeng Kunshan, Jiangsu, CN 1 1
ZENG, Zuoxiang Shanghai, CN 8 4
ZHU, Wanyu Shanghai, CN 7 4

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