PREPARATION METHOD FOR MOISTURE-CURING POLYURETHANE REACTIVE HOT MELT ADHESIVE FOR TEXTILE COMPOSITION
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Aug 28, 2014
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Sep 26, 2013
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Abstract
A preparation method for moisture-curing polyurethane reactive hot melt adhesive for textile lamination mainly includes the following steps: (1) mixing and stirring polyether polyol 4000E, polyester polyol 3000H, polyester polyol 2000N, and an antioxidant, heating the mixture to about 120° C., and dehydrating for 0.5h under a vacuum of lower than 100 Pa; (2) adding a tackifying resin, heating the mixture to 135-140° C., and dehydrating for 1.5h under a vacuum of lower than 100 Pa; (3) lowering the temperature to 87° C., adding 4,4′-diphenylmethane diisocyanate and a catalysis, stirring the mixture, and reacting for 2h under a vacuum of lower than 100 Pa; (4) releasing vacuum, adding white carbon black, rapidly stirring the mixture evenly, and further stirring for 10 min under a vacuum of lower than 100 Pa; and (5) rapidly discharging at a temperature of 85-100° C., packaging, and then curing for 4h at 80-85° C., to obtain a target product. When applied in textile lamination, the product exhibits excellent peel strength, a relatively short open time, good hydrolysis resistance and desirable storage stability.

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- 15 United States
- 10 France
- 8 Japan
- 7 China
- 5 Korea
- 2 Other
Patent Owner(s)
Patent Owner | Address | |
---|---|---|
EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY | SHANGHAI 200237 | |
SHANGHAI TIANYANG HOT MELT ADHESIVE CO LTD | 505 HUIPING ROAD JIADING DISTRICT SHANGHAI 201802 | |
KUNSHAN TIANYANG HOT MELT ADHESIVE CO LTD | QIANDENG TOWN WENPU ROAD KUNSHAN CITY SUZHOU CITY JIANGSU PROVINCE 215341 NO 366 SUZHOU CITY JIANGSU PROVINCE 215341 |
International Classification(s)

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- [Patents Count]
Inventor(s)
Inventor Name | Address | # of filed Patents | Total Citations |
---|---|---|---|
LI, Zhelong | Shanghai, CN | 10 | 6 |
MA, Hongwei | Shanghai, CN | 86 | 273 |
SHEN, Yan | Shanghai, CN | 51 | 608 |
XIAO, Hupeng | Kunshan, Jiangsu, CN | 1 | 1 |
ZENG, Zuoxiang | Shanghai, CN | 8 | 4 |
ZHU, Wanyu | Shanghai, CN | 7 | 4 |
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11.5 Year Payment | $7400.00 | $3700.00 | $1850.00 | Jan 28, 2028 |
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Surcharge - 11.5 year - Late payment within 6 months | $160.00 | $80.00 | $40.00 |
Surcharge after expiration - Late payment is unavoidable | $700.00 | $350.00 | $175.00 |
Surcharge after expiration - Late payment is unintentional | $1,640.00 | $820.00 | $410.00 |
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