METHOD FOR MAKING HIGH PURITY DICYCLOPENTADIENE
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United States of America Patent
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Jun 25, 2015
app pub date -
Aug 28, 2014
filing date -
Dec 24, 2013
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Abstract
A method for making high purity dicyclopentadiene comprises the following steps: providing a dimer feedstock comprising dicyclopentadiene and methyl dicyclopentadiene; blending the dimer feedstock and a diluent to obtain a first blend; cracking the first blend in a vapor phase at 300° C. to 400° C. to obtain a cracked feedstock; separating the cracked feedstock into a second blend and a third blend; dimerizing the second blend at 50° C. to 120° C. to obtain a fourth blend; and separating the fourth blend to obtain a recycled diluent and high purity dicyclopentadiene. By using saturated C5 hydrocarbon, saturated C6 hydrocarbon, benzene and the mixture thereof as the diluent and the steps mentioned above, the clogging problem of cracker tubes is solved and the cost of makeup diluent usage is lowered.
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