METHOD OF PREPARATION OF ALANE-ETHERATE AND ALANE
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United States of America Patent
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Issued Date -
Apr 2, 2015
app pub date -
Dec 2, 2014
filing date -
Jun 5, 2012
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Abandoned
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Abstract
The invention to preparing alane-etherate and alane by producing an alane-etherate complex using an acid including one or a combination of hydrochloric acid and methanesulfonic acid and a metal tetrahydroaluminate in a solvent including an ether such as diethyl ether. The alane-etherate can be desolvated using a spray desolvation process such as electrospraying.
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