Apparatus and Method for Providing Low Temperature Reaction Conditions
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United States of America Patent
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Issued Date -
Apr 4, 2013
app pub date -
Feb 17, 2011
filing date -
Feb 19, 2010
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Abandoned
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Abstract
A reaction vessel for conducting low temperature reactions is disclosed, the reaction vessel comprising: a circulation chamber with an entry port for the supply of a cooling medium at a temperature below ambient to said circulation chamber and an exhaust port; and a reaction chamber and a centrifugal fan arranged concentrically-inside the circulation chamber so that gas in said circulation chamber is forced radially outwards by the operation of said fan, wherein the movement of the gas past the reaction chamber maintains the temperature of reactants inside the reaction chamber at a temperature below ambient. A chiller for providing a gas supply at a temperature below ambient is also disclosed which may be used with the above reaction vessel.
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