NITRATION OF ACTIVATED AROMATICS IN MICROREACTORS
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United States of America Patent
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Issued Date -
Nov 25, 2010
app pub date -
Jan 12, 2006
filing date -
Jan 12, 2006
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Abstract
The invention relates to the nitration of aromatic or heteroaromatic compounds, wherein an activated aromatic or heteroaromatic compound and a nitration agent, optionally in the presence of a solvent, are mixed intensely in a microreactor, and wherein the proportion of the nitration agent to the activated aromatic or heteroaromatic compound, the concentration of nitration agent in the reaction mixture, and the temperature are selected at levels such high that the nitration begins autocatalytically, and wherein the nitration product is obtained after leaving the microreactor and, optionally after an after-reaction time outside the microreactor.
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