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Abstract

Method and device for the preparation of monophasic powders of actinide salts which are precursors in the production of fuel pellets. In one aspect, a compact and simple device is provided to obtain dry monophasic powders of actinide salts in one stage, while increasing the productivity, chemical and nuclear safety of the process. In a second aspect, the method comprises feeding of nitric actinides-containing solution and formic acid to a cylindrical heated reactor, grinding the resulting powder, and discharging the powder. The nitric actinides-containing solution and formic acid are continuously metered to the upper zone of the reactor so that the reactive chemicals are mixed in a thin film on the heat-exchange surface, where the reaction mixture is continuously stirred by rotor blades. Also occurring are the processes of denitration, formation of the relevant compounds, their drying and grinding and collecting dry salts of actinides in a hopper by gravity.

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